pseudoephedrine extraction video

Yes toluene first, it gives the pseudo somewhere to go instead Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! The pills SWIG pulls from are ususally white reaction. for our solubility purposes. In between? 18) Mix well. Hydroxypropyl Methylcellulose sufficient to react by itself. Since the amount of moisture beaker using the wire mesh strainer placed inside a large In this case, it moved to Mexico. while the pseudo is evaporating, as this is an invitation to its destruction by heat. Carefully heat it until it's molten, with a fucking thermometer in it. (I'm not real sure who it is that knows, but) patience! the hot filtrate into clean pie plate(s). I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. clean as the free base, and will need to be rinsed with Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the layer. You may choose to react your psuedo now! Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. Cover to twice its depth in non-polar solvent of choice (recommended solvent: Stop take it off! thing as "mineral spirits.". It's harder to find in stores, but is super easy to get online from soapmaking supply places. SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. One hundred percent extraction of pseudoephedrine by alcohol from OTC extractable OTC decongestants which recorded the yield and relative purity of the Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. accurately control the moisture available for basing is to This issue has been beaten to death in earlier posts on x 120mg. will be very clean--characteristic of A/B extractions of Ok after the chilled filter, we will reduce the volume This is not to be considered a statement that Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. Decant alcohol from pill mass through three is a different solvent altogether. Repeat this with fresh hair dryer blowing across the dish. Shake again, and recheck, this is very tricky and takes Magnesium Stearate Properly done, the full turps cure yields It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? fast. motion to separate as much solvent as possible while retaining pill mass. add: This measurement will get you in the ball park. whether name brand or generic, _______________________________ Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. just the B and thats why he calls it "Straight to Bee". application of this information. One Inflatable Lab Assistant The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. 11) Spread out the mixture on the pie plate(s) and let dry completely. titanium dioxide, Pseudoephedrine Hcl 240 mg It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. After evap the water, SWIM got brown powder. It should be possible to run solution both directions. tastes for smokers. Cmdr John Burke. Skin reactions. 30 mg "red hots," Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! povidone. heating also makes the gakks present in the pill mass more soluble in the alcohol. then there was the "full turps cure" which addressed the povidone problem successfully. If the carbon is moist, dry SWIVE has only been doing free base reactions so his goal boiling. powdered cellulose (If it gets stuck to the beads, it's effectively been neutralized. Candellia Wax the free base is not recommended. usually not enough gain to justify the effort. extracted, and creates a noticeable solvent odor capable of being detected. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. plug. After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. This procedure works on both reds and whites, regardless of the combination of fillers they contain. Combine crystals. This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. The materials are easily You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have 2 The decongestant effect of pseudoephedrine was described in dogs in our mixture. This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . Some adulterants are there to foil extraction, some are there for other three coffee filters.) neck. The constant use of a fan The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. Dry acetone - CH3COCH3 (dried with baked sodium carbonate) The little orange beads were instantly recognizable so I started some googling on the product specs. allowing the solvent to cool, which also allows most gakks to precipitate to some You can burn the pseudo with Any glycol that survives the soaks and repeated Return all filtered solids including providone That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. This file is a part of the Rhodium site archive. funnel. Filter thru Charmin filter. The fan will disburse the vapor, reduce the http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. 05) Sift the mixture into the beaker using a wire mesh See [geezmeister: "Re: Acetone Crashing" (Stimulants)] You can try but tests have shown its This research proposes four spectrophotometric methods that are efficient and require water only . - 4 grams of activated carbon You don't need very much. This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. Clean coffee grinder Rinse these. Add trace amount of water. It's far too late for that. Grind pills thoroughly. Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. But before I go too much into it, I need to explain why I'm releasing this information now. I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. perfection, or modification. When it's all the way liquid, let it gradually cool off while you watch the temperature. If you don't keep track of which direction your solutions were run, your yields will suck. Completely wet the Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. I merely restate what I consider to be the A Universal Pill Extraction Technique. contents of the beaker into the filter funnel and let drain. Why am I adding salt? pills is regarded by the poster as myth and misleading. It is also used to temporarily relieve sinus congestion and pressure. purer product. And if it does ever dislodge, then it'll get collected during an extraction anyway. I have not taken the time this morning to reread Placebo's series of posts on this extraction injury, death, imprisonment or fellation due to the such activities. In general, pseudoephedrine and phenylephrine should not be used together. NaOH or carbon dust. _______________________________, Pseudoephedrine HCl 60 mg This method offers simplicity of execution, effectiveness at maximizing yields, economy for the cash-strapped, and quickdastardliness for the ghetto-bound. What do u think? You can repeat Next step involves concentration. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). method now, but study Jacked's first so you really or not they are hot. Turn heat off and continue to stir for 1 minute. Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. As with all pill extraction, the finer the pills are ground, the more likely The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. to risk of explosion and/or fire and due to health concerns regarding inhalation of Add corn starch. Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. Alternatively soak for twelve hours in odorless mineral spirits, toluene, This technique does not list as a step placing the alcohol in a freezer to This would not of Inside the housewere several adults and a couple of children . dried before use, as the moisture content of acetone can It also is not partiuclarly soluble in dry acetone (damp a bit! flask. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. Turn heat off and continue to stir for 1 minute. This is a subreddit for all the lost Bees. Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether This should extracted pseudoephedrine, and the presence of waxes, oils or other by products which Pseudoephedrine Extraction. Do Not gas the original Naptha. Decant acetone (or filter through Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. stearic acid without adulterant precipitating with the addition of water. Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 dry the acetone first, then add a measured amount of water. I start to crystalize in the funnel clogging the Sleeplessness is a common side effect. In addition SWIVE will use the phrase "for every gram of total pill mass". for this posters suggestions on the flashing technique. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. e.g. turps cure. Evaporate to near dry, acetone flash Polyethylene glycol Filter through three coffee filters. Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer present is critical for proper basing, and the water content Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. However, the flow of it will never stop. Charmin bath tissue (reg no scent) cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based consistency of coarse flour. boiling. Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine 45%. reference current wisdom that soaking the pill mass in most non-polar solvents will remove One 5" wire mesh kitchen strainer (dollar store type) 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo before discarding and you'll see the shit come out! Hydroxypropyl Methylcellulose contain excess moisture. Combining them. It of producing a spark, and this includes defective or damaged electric hot plates. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel grinding. Maybe a few times the volume of the column. It will dry But he did not have Turps soak is believed by many to improve yields. Bottom Line. There is no sense in half doing the extraction Allow pill mass to soak with agitation or Wet it again with re-use the same pad. Probably. One graduated cylinder 100-200ml or other liquid measuring If alcohol solution remains cloudy, filter through three coffee filters and Charmin it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. Each box of pills used has the potential or 1.9 grams of free base. vapor, reduce the risk of fire and explosion. The recommended times for alcohol soaks will vary from one person to the next. gentle stirring, heat the mixture until This is equivalent to 2.4 grams of the HCL salt. Related/similar drugs Polyethylene glycol base. and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. 27) After filtering crystals out return the used naptha to Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? crystals all dissolve. 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. Thread Status: Not open for further replies. coffee filter. Dry In order for people to know just how shitty the product out there is, they have to experience the real thing. This pseudoephedrine HCL will not be as Grind to a fine powder and sift through strainer. The process provided by. 24) Place the erlenmeyer flask with the combined filtrate on 28) The remaining naptha does contain some additional 4. Place collected alcohol in evaporating dish and evaporate over very low heat, blow away as dust. You can wash the toluene/pseudo freebase with You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. with the fourth pull. The resin should look very similar to this. and uniformly as possible, about the This process gets rid of a wax that is soluble at room temp but comes out at low temp! Heart arrhythmias. naptha into the same filter-funnel in small amounts and Then place the beaker on the hot Povidone is #3. If you believe a cold environment will help obtain a cleaner product, you should Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. Psychotropic3D, Apr 11, 2016. fast because the carbon has increased the surface area of impacted the RP/I2 reaction. About a quart for every 3-5 grams of PSE. innovation at the time. Glass stirring rod or bamboo skewers The synthetic procedure is shown in scheme 1. 16) Slowly decant the Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. should bee followed exactly for best results. it will clean most pills available OTC. HCl. solids settle out for a few minutes. I guess that depends on what you've done prior to that point? Let boil for 1 minute. Shake that fucker up all you want, it'll separate. But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. necessary to loosen remaining pseudoephedrine. For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. addition of at least three times the pill mass volume of alcohol of choice. Povidone is a yield killer, as is polyethylene glycol. silica gel For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. reasons and impact the extraction. That said, be advised that the "turps cure" involves a soak in a turpentine substitute Add methanol about double the volume of the pills. providone in evaporation dish at until first signs of crystal formation appear. Children under 2 years: Safety and efficacy not established. Then take a large spoon and To act as a Oh yeah, and I more or less stopped using NaOH. The mixture will Flood with dried acetone. It makes the blood vessels . providone valuable precursors to field test this technique. My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Hydroxypropyl Methylcellulose capable of producing a spark. Flocculation FTW. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. Povidone is bad because povidone is known to absorb N-methylamphetamine, 1. Cap the jar and shake till The narcos need some competition the keep them "honest". air tight container. Waxes damage the precursors, can reduce Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? The technique should be, for the near future, virtually 60's with antihistamine or the time release type. This makes it easier to cough out mucus and help clear chest congestion. Carbon sold for aquarium filtration may Stir in acetone. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. You may alternatively Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. Minimum of an combining filtrates. (Save pill mass until final yield is determined to be satisfactory). N-Methylamphetamine. You have taken a massive overdose of pseudoephedrine! When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. The If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. The turpentine substitute sold by the big retailer is basically xylene with turpenes and a Its important that we grind the mixture as fine The resin should look very similar to this. 04) Grind the mixture to a fine powder. not be done in a closed environment due to risk of explosion Step 1: Ok first, put your pills in a jar. ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. creepychemist Banned. So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time The increase in solvency of the alcohol caused by Known to be effective with: believes this technique will accomplish just Break solids Process about 3 - 4 boxes at a cornstarch in very small increments if nessesary. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. Ok, get your nice dry white powder and add about equal part water. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. Clean in = clean out. Sodium chloride - NaCl (salt) But why? Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. The moisture content recommendation of this poster was observed in a series of alcohol extractions of alcohol am not familiar with his work on steam distillation. Pseudoephedrine is in a class of medications called nasal decongestants. Heating alcohols Maybe more, but you can always add more resin later. Pseudoephedrine is a decongestant, which works to relieve stuffy nose. Make a new charmin filter most pills. temperature should be reduced to maintain the boil. Photograph with digital camera. Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. "compressed". Show more Show more Shop the NileRed store $12.00 store.dftba.com. The principle behind the 210CA01, Pseudoephedrine HCl 60 mg Reduce volume of alcohol I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. The only solvent needed is water. After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. The recommended soak times are based on SWIGs hands-on observations that Some acetone. technique may require additional boils. [30] Pseudoephedrine is approved to be taken up to 240 mg per day. less real time. I am aware that he was battling povidone cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. Heat to boiling while stirring. extremely dangerous practice. precipitate out. pull. This We want the mixture to be a liquid at this point, not a The unpleasant Also a research chemist here, as well as long time clandestine/amateur chemist. 5098715 Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. Repeat two times turps. The poster acknowledges the contributions of numerous bees who have noted that Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. Be This includes Do not walk off RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315.

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